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4. On the left hand portion of the window, select Routine Editor.
5. Hit Reset in the lower right hand corner of the window.
6. If a method needs to be created, select New and create a program for the TGA (for
specifics on creating a new Method, please refer to the person/s in charge of the
instrument). If a method is already created, select it using the Open tab.
The pans used are 40 µL aluminum pans with a pin on the bottom. The pin allows
for accurate sample placement on the sensor. Each pan contains two parts: the
bottom with the pin and the hat.
Prior to running a DSC, knowledge of the decomposition temperature, T
d
, is
beneficial. This will allow you to run a method that ramps up to the highest
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